[proof]
*Step 1. Case $s > n$.*
Fix $\varepsilon > 0$.
Because $E$ is a subset of $\mathbb R^{n}$, there exists a countable collection of closed cubes $\{Q_{k}\}_{k=1}^{\infty}$ that covers $E$ and satisfies
\begin{align*}
\sum_{k=1}^{\infty}\lambda^{n}(Q_{k}) < \varepsilon.
\end{align*}
For each $k$, the diameter $\operatorname{diam}Q_{k}$ equals the edge length $l_{k}$ times $\sqrt n$.
Therefore
\begin{align*}
\sum_{k=1}^{\infty}(\operatorname{diam}Q_{k})^{s}
=(\sqrt n)^{s}\sum_{k=1}^{\infty}l_{k}^{s}
\le(\sqrt n)^{s}\sum_{k=1}^{\infty}l_{k}^{n}
=(\sqrt n)^{s-n}\sum_{k=1}^{\infty}\lambda^{n}(Q_{k})
< (\sqrt n)^{s-n}\varepsilon.
\end{align*}
Since $\varepsilon$ was arbitrary, $\mathcal H^{s}(E)=0$.
*Step 2. Case $s < n $ with $\operatorname{int}E\neq\varnothing$.*
Choose a closed ball $\overline B_{r}(x_{0})\subset E$.
For any cover $\{A_{k}\}$ of $E$ with $\operatorname{diam}A_{k} < \delta$, the same family covers $\overline B_{r}(x_{0})$.
Each set $A_{k}$ lies inside some ball of radius $\operatorname{diam}A_{k}$, so the volume of $A_{k}$ is bounded above by $c_{n}\operatorname{diam}(A_{k})^{\,n}$, where $c_{n}$ is the volume of the $n$-dimensional unit ball.
Because the volumes of the $A_{k}$ sum to at least the volume of $\overline B_{r}(x_{0})$,
\begin{align*}
c_{n}r^{n}\le
\sum_{k=1}^{\infty}c_{n}\operatorname{diam}(A_{k})^{\,n}.
\end{align*}
Hence
\begin{align*}
\sum_{k=1}^{\infty}\operatorname{diam}(A_{k})^{s}
\ge\sum_{k=1}^{\infty}\operatorname{diam}(A_{k})^{\,n}
\ge r^{n}.
\end{align*}
The right side is independent of $\delta$, so $\mathcal H^{s}_{\delta}(E)\ge r^{n}$ for every $\delta$.
Consequently $\mathcal H^{s}(E)=\infty$.
*Step 3. Identification with Lebesgue measure when $s=n$.*
First assume $E$ is an open cube $Q$.
For any $\delta > 0$ the cover consisting solely of $Q$ shows
$\mathcal H^{n}_{\delta}(Q)\le(\operatorname{diam}Q)^{n}=n^{n/2}\lambda^{n}(Q)$.
Conversely, if $\{A_{k}\}$ covers $Q$ with $\operatorname{diam}A_{k} < \delta$, Vitali’s covering theorem produces a finite subcollection of disjoint balls $\{B_{k}\}_{k=1}^{m}$ such that the union of the concentric balls $5B_{k}$ still covers $Q$.
The diameter of $5B_{k}$ equals $5\,\operatorname{diam}B_{k}$, and the disjointness implies
\begin{align*}
\lambda^{n}(Q)\le\sum_{k=1}^{m}\lambda^{n}(5B_{k})
=5^{n}\,\omega_{n}\sum_{k=1}^{m}r_{k}^{\,n}
\le 5^{n}\,\omega_{n}\sum_{k=1}^{m}(\operatorname{diam}B_{k})^{n}.
\end{align*}
Because $\operatorname{diam}B_{k}\le\operatorname{diam}A_{k}$, this yields
\begin{align*}
\lambda^{n}(Q)\le 5^{n}\,\omega_{n}\sum_{k=1}^{\infty}(\operatorname{diam}A_{k})^{n}.
\end{align*}
Taking the infimum over all admissible covers and then the limit $\delta\downarrow0$ gives
\begin{align*}
\lambda^{n}(Q)\le 5^{n}\,\omega_{n}\,\mathcal H^{n}(Q).
\end{align*}
Combining the two bounds yields
\begin{align*}
c_{n}^{-1}\lambda^{n}(Q)\le\mathcal H^{n}(Q)\le c_{n}\lambda^{n}(Q)
\quad\text{with }c_{n}=\max\bigl\{n^{n/2},5^{n}\omega_{n}\bigr\}.
\end{align*}
A standard outer regularity argument extends the equality $\mathcal H^{n}=c_{n}\lambda^{n}$ from cubes to all Borel sets.
[/proof]